额.........俺是来求助的

凉秋-人淡如菊UID: 2587559

发工版么人理我..........= =
还是发水版来

江湖救急!!!
请各位大虾鼎力相助
柒某将感激不尽

翻译 -
染色时遇铜,铁离子色光均有变化.以1,5-二羟基蒽醌和苯酚,苯甲醚为原料,首先将1,5-二羟基蒽醌磺化,硝化,还原得1,5-二羟基-4,8-二氨基蒽醌-2,6-二磺酸钠,再将其分别与苯酚,苯甲醚进行加成转位反应,最后将磺酸基水解即得产物.经过滤,水洗至中性,研磨,干燥即得产品.
将1份1,5-二羟基蒽醌,13.98份发烟硫酸,0.35份无水硫酸钠,于110~115摄氏度;C进行磺化反应4小时,用6.92份硫酸稀释.磺化稀释物与配置好的混酸[由4.73kg硝酸(95%),9.7kg硫酸(96%)及1.9kg水配置而得]混合,升温至55~60摄氏度;C进行硝化反应后,降温,过滤.取47.2kg硝化滤饼,8.25kg硫化钠(100%),于75~78摄氏度;C进行还原反应1.5~2小时后,压滤,用食盐加碱溶液洗至无硫化钠为止,得1,5-二羟基-4,8二氨基蒽醌-2,6-二磺酸钠(I).

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自己OK了
可是这银子给谁好。。。。。。。。= =

================
发完~:loveliness:

yy_jessyUID: 2582341

额。。。。。
组织上对此行为给予高度的认可与表扬！
全体起立
呱唧！
凉秋-人淡如菊 发表于 2009-7-23 22:38

这个...是吧...纵观几个楼层的发言，组织貌似就咱俩银儿啊...

SpectoriaUID: 2488330

:funk:大姑。。。拜服鸟Orz

凉秋-人淡如菊UID: 2587559

我一上午都在搞这个
都快吐了
我又不是学化工的..........= =

阿泰UID: 209473

jialiangleoUID: 2307941

SpectoriaUID: 2488330

:L

凉秋-人淡如菊UID: 2587559

就没个学化工的人来帮我搞定哈子啊

凉秋-人淡如菊UID: 2587559

谁帮忙搞顶
男的给介绍美女
女的给介绍帅哥

ahleeUID: 2188425

....惊为天人！！

凉秋-人淡如菊UID: 2587559

我继续折腾
我已经折腾到这一断了
折腾好拿出来大家共'赏'之

节俭的D同学UID: 2625249

来围观

凉秋-人淡如菊UID: 2587559

The color light change when meet Cu, Fe ion during dyeing. Use the 1,5-dihydroxyanthraquinone, phenol and anisole as the raw material. First, sulphonate and nitrify 1,5-dihydroxyanthraquinone to get the intermediate 1,5-dihydroxyl-4,8-diamidoanthraquinone-2,6-disulfonate. Then the intermediate react with phenol and anisole, hydrolyze the sulphonic group to get product. Get the final production through filtration, watering till neutral, grinding and dryness.

1mol 1,5-dihydroxyanthraquinone, 13.98mol oleum and 0.35mol anhydrous sodium sulphate, sulphonate at 110~115ºC for 4 hours and then dilute with 6.92mol sulfate. Commix the sulphonated diluent with the mixed acid [4.73kgnitric acid (95%), 9.7kg sulfate (96%) and 1.9kg water], then cool and filtrate after heating up to 55~60ºC to get press cake. 47.2kg nitrified press cake react with 8.25kg Sodium sulfide (100%) at 75~78ºC for 1.5~2 hours, then get the 1,5-dihydroxyl-4,8-diamidoanthraquinone-2,6-disulfonate(I) after pressure filtration, counteracting sodium sulfide with salt and aqueous alkali completely.

我继续
大家围观

sacredno1UID: 208290

A大师不懂？不是学这个相关的吗

凉秋-人淡如菊UID: 2587559

A大师不懂？不是学这个相关的吗
sacredno1 发表于 2009-7-23 15:33

他是环境的
俺这个是化工

哎~~上次做环境报告,他都不鸟我啊
自己搞定
继续受折磨